Mark Hail: Publications, Patents, and Presentations
Publications Molecular Weights of CTLA-4 and CD80 by Sedimentation Equilibrium Ultracentrifugation, R. Fairman; W. Fenderson, M. E. Hail, Y. Wu, S. Shaw, Analytical Biochemistry, 270(2), 286-295, (1999). Use of affinity capillary electrophoresis for the study of protein and drug interactions; J. Liu, S. Abid, M. E. Hail, M. S. Lee, J. Hangeland, N. Zein; Analyst, 123(7), 1455-1459, (1998). Recent applications of LC-MS techniques for the structure identification of drug metabolites and related compounds; M. S. Lee, E. H. Kerns, M. E. Hail, J. Liu, K. J. Volk; LC-GC, 15(6), 542, 544, 546, 548, 550, 552, 554, 556, 558, (1997). "Stimulation of Activin A Expression in Rat Aortic Smooth Muscle Cell by Thrombin and Angiotensin II Correlates with Neointimal Formation In Vivo"; John E. Pawlowski, David S. Taylor, Maria Valentine, Mark E. Hail, Patricia Ferrer, Mark C. Kowala, and Christopher J. Molloy; J. Clin. Invest., 100(3), 639-648, (1997). "Presence of Glycerol Masks the Effects of Phosphorylation on the Catalytic Efficiency of Cytosolic Phospholipase A2"; J. R. Burke, M. G. Guenther, M. R. Witmer, J. A. Tredup, M. E. Hail, R. Micanovic, J. J. Villafranca; Archives of Biochemistry and Biophysics, 341(1), 177-185, (1997). "Structural Studies of Escherichia coli UDP-N-Acetylmuramate:L-Alanine Ligase"; H. Jin, J. J. Emanuele, R. Fairman, J. G. Robertson, M. E. Hail, H. Ho, P. J. Falk, J. J. Villafranca; Biochemistry, 35(5), 1423-1431, (1996). "Active Recombinant Human Cytosolic Phospholipase A2 is Expressed in Escherichia coli"; M. R. Witmer, R. Micanovic, J. Tredup, W. Lin, M. E. Hail, J. J. Villafranca; Archives of Biochemistry and Biophysics, 318(2), 430-438, (1995). "In vitro Proteolytic Activity and Active-site Identification of the Human Cytomegalovirus Protease"; J. T. Stevens, C. Mapelli, J. Tsao, M.E. Hail, D. OíBoyle, S. P. Weinheimer, and C. L. DiIanni; Eur. J. Biochem, 226, 361-367 (1994). "Rapid High-sensitivity Peptide Mapping by Liquid Chromatography-Mass Spectrometry"; K. Mock, M. Hail, I. Mylchreest, J. Zhou, K. Johnson, I. Jardine, J. Chromatogr., 1993, 646(1), 169-174. "Electrospray Ionization for Analysis of Platelet-activating Factor", S. T. Weintraub, R. N. Pinckard, and M. E. Hail, Rapid Comm. Mass Spectrom., 1991, 5, 309-311. "Detection and Sequence Analysis of Tryptic Peptides by Microcolumn Liquid Chromatography-Tandem Mass Spectrometry Using an Electrospray Interface", M. Novotny, J. Liu, M. E. Hail, S. Lewis, I. Jardine, J. Microcol. Sep., 1990, 2, 285-292. "Biological Mass Spectrometry", A. L. Burlingame and J. A. McCloskey, eds., Proc. of the 2nd Int. Symp. on Mass Spectrom. in the Health and Life Sciences, 1990,101-118, Chapter 6: Analysis of Peptides and Proteins by Tandem Quadrupole Mass Spectrometry, M. Hail, S. Lewis, J. Zhou, J. Schwartz, I. Jardine, and C. Whitehouse. "Current Research in Protein Chemistry: Techniques, Structure, and Function", J. J. Villafranca, ed., 1990, 105-116, Chapter 10: Analysis of Peptides and Proteins by Tandem Quadrupole Mass Spectrometry, M. Hail, S. Lewis, J. Zhou, I. Jardine, and C. Whitehouse. "Estimation of Mutagenic/Carcinogenic Potential of Environmental Contaminants by Ion-Molecule Reactions and Tandem Mass Spectrometry ", J. A.. Freeman, J. V. Johnson, M. E. Hail, D. W. Kuehl, and R. A. Yost, J. Amer. Soc. Mass Spectrom.,1990, 1, 110-115. "Gas Chromatographic Sample Introduction into the Collision Cell of a Triple Quadrupole Mass Spectrometer for MassSelection of Reactant Ions for Charge Exchange and Chemical Ionization ", M. E. Hail, D. W. Berberich, and R. A. Yost, Anal. Chem.,1989, 61, 1874-1879. "Theoretical and Practical Aspects of Short Open Tubular Columns at Subambient Pressures in Gas Chromatography/Mass Spectrometry", M. E. Hail and R. A. Yost, Anal. Chem.,1989, 61, 2402-2410. "Compact Gas Chromatograph Probe for Gas Chromatography/Mass Spectrometry Utilizing Resistively Heated Aluminum-Clad Capillary Columns", M. E. Hail and R. A. Yost, Anal. Chem.,1989, 61, 2410-2416. "Mass-Selection of Reactant Ions for Chemical Ionization in Quadrupole Ion Trap and Triple Quadrupole Mass Spectrometers ", D. W. Berberich, M. E. Hail, and R. A. Yost, Int. J. Mass Spectrom. Ion Proc.,1989, 94, 115-147. "High-Precision Automated Conductometric Titrations with the Bipolar Pulse Technique", M. E. Hail and F. J. Holler, Mikrochimica Acta, 1986 III, 295-308. Patents "Method and apparatus for focusing ions in viscous flow jet expansion region of an electrospray apparatus", U.S. Patent # 5,157,260, Oct. 20, 1992, I. C. Mylchreest, M. E. Hail, J. R. Herron, assigned to Finnigan Corp., San Jose, CA. "Electrospray ion source with reduced neutral noise and method", U. S. Patents #5,171,990, Dec. 15, 1992, # RE35,413, Dec. 31, 1996, I. C. Mylchreest and M. E. Hail, assigned to Finnigan Corp., San Jose, CA. "Electrospray ion source and interface apparatus and method", U. S. Patents # 5,170,053, Dec., 8, 1992, #5,393,975, Feb., 28 1995, M. E. Hail, I. C. Mylchreest, assigned to Finnigan Corp., San Jose, CA, Analytica, Branford, CT. "Multilayer flow electrospray ion source using improved sheath liquid", U.S. Patent # 5,122,670, May 17, 1991, I. C. Mylchreest and M. E. Hail, assigned to Finnigan Corp., San Jose, CA. "Direct resistive heating and temperature measurement of metal-clad capillary columns in gas chromatography and related separation techniques", U. S. Patent # 5,114,439, May 19, 1992, R. A. Yost, and M. E. Hail, assigned to the University of Florida, Gainesville, FL. Presentations
"Improved Methods for Totally Automated Analysis, Data Processing, and Results Reporting in Biomolecule LC/MS", Mark E. Hail, Jeffrey L. Whitney, David J. Detlefsen, 50th ASMS Conference on Mass Spectrometry and Allied Topics, Orlando, FL, June 2002.
"Automated LC/MS Analysis of Biomolecules Using ProMassXcali", Mark E. Hail, Jeffrey L. Whitney, ABRF 2002, Austin, TX, March 2002. "Characterization and Detailed Analysis of Oligonucleotides and Proteins by LC/MS", Jeffrey L. Whitney, Mark E. Hail, ABRF 2002, Austin, TX, March 2002. "Automated LC/MS Analysis of Biomolecules Using ProMass", Mark E. Hail, Jeffrey L. Whitney, 4th Annual Symposium on Chemical and Pharmaceutical Structure Analysis, Princeton, NJ, October 2001. "Automated LC/MS Profiling of Proteins Using the ProMass Protein Molecular Weight Data Browser", Mark E. Hail, Jeffrey L. Whitney, 49th ASMS Conference on Mass Spectrometry and Allied Topics, Chicago, IL, June 2001. "High Throughput Compound Integrity Checking Using Data-Dependent SMARTLCMS", Mark Hail, Mark Sanders, 48th ASMS Conference on Mass Spectrometry and Allied Topics, Long Beach, CA, June 2000. "Strategies for Automated On-line and Off-line Detergent Removal in the Mass Spectrometric Analysis of Proteins", Haiying Zhang, Mark Hail, Brent Kleintop, Kevin Volk, 47th ASMS Conference on Mass Spectrometry and Allied Topics, Dallas, TX, June 1999. Organized and chaired a session at the Eastern Analytical Symposium (EAS) entitled "Recent Advances in Mass Spectrometric Analysis of Biomolecules", November, 1998. "Strategies for Rapid Protein Identification and Characterization Using Automated Ion Trap MS/MS and Database Searching" Mark E. Hail, Mark Sanders, Michael L. Nedved, Iain C. Mylchreest and Mike S. Lee, Eastern Analytical Symposium, Somerset, NJ, November 1998. "Automated Mass Spectrometric Strategies for Accelerating Drug Discovery and Development"; Mark E. Hail, keynote address at Finnigan MAT Users Forum, 45th ASMS Conference on Mass Spectrometry and Allied Topics, Palm Springs, CA, June 1997; Laboratory Automation í98, San Diego, CA, January 1998; Chicago Area Mass Spec Discussion Group, April, 1998; Finnigan MidAtlantic Users Meeting, Langhorne, PA, October, 1998. "Predictive Degradation Profiling of Biomolecules using LC/MS Methodologies", Brent Kleintop, Kevin Volk, Chris Reddick, Mark Hail, Mark Sanders, David Detlefson, Ed Kerns, Mike Lee, 46th ASMS Conference on Mass Spectrometry and Allied Topics, Orlando, FL, June 1998. "The Role of LC/MS/MS Spectral Library Searching for Impurity Analysis Using Ion Trap and Triple Quadrupole Mass Spectrometers" Jonathan Josephs, Mark Sanders, Mark Bolgar, Gerald DiDonato, Mark Hail, Ed Kerns, Mike Lee, 46th ASMS Conference on Mass Spectrometry and Allied Topics, Orlando, FL, June 1998. "The Effect of Mobile Phase Modifiers on the Observation of H2SO4 Adducts to Proteins During ESI LC/MS", Bethanne Warrack, Mark Hail, 46th ASMS Conference on Mass Spectrometry and Allied Topics, Orlando, FL, June 1998. "Probing Protein Structure Using On-line Deuterium Exchange ESI/MS"; Mark E. Hail, J. David Cox, David J. Detlefsen, Mike S. Lee; 45th ASMS Conference on Mass Spectrometry and Allied Topics, Palm Springs, CA, June 1997. "An Integrated Approach to Biomolecule Analysis: Automated LC/MS with Data-dependent Fractionation for MALDI/MS"; Mark E. Hail, Mark Sanders, Bethanne M. Warrack, Jeffrey L. Whitney, Michael L. Nedved, Mike S. Lee; 45th ASMS Conference on Mass Spectrometry and Allied Topics, Palm Springs, CA, June 1997. "Accelerated Identification and Characterization of Metabolites by LC/MS Using On-Line Sample Clean-Up and Automated MS/MS"; Michael L. Nedved, Mark Sanders, R. Gedamke, G. DiDonato, M. Hail, R. Kammerer, Mike S. Lee; 45th ASMS Conference on Mass Spectrometry and Allied Topics, Palm Springs, CA, June 1997. "Fully Automated Protein Identification: On-line Digestion, m-LC, Ion Trap MS/MS, and Database Searching;" Mark Sanders, Michael L. Nedved, Mark E. Hail, Mike S. Lee; 45th ASMS Conference on Mass Spectrometry and Allied Topics, Palm Springs, CA, June 1997. "Deconvoluting Structural Trends in Biomolecular LC/MS Datasets Using Scientific Visualization"; J. L. Whitney, M. E. Hail, M. L. Nedved, M. Sanders, K. J. Volk, E. H. Kerns, M. S. Lee; 45th ASMS Conference on Mass Spectrometry and Allied Topics, Palm Springs, CA, June 1997. "Investigation of Precursor Ion Scanning for the Improved Detection of Proteins in the Presence of Non-ionic Surfactants"; Bethanne M. Warrack, Mike S. Lee, Mark E. Hail; 45th ASMS Conference on Mass Spectrometry and Allied Topics, Palm Springs, CA, June 1997. "Automated LC/MS/MS and CID Spectral Library Searching of Steroids Using Ion Traps and Triple Quads"; Jonathan Josephs, Mark Sanders, Gerald DiDonato, Mark Hail, Edward Kerns, Kevin Volk, and Mike Lee; 45th ASMS Conference on Mass Spectrometry and Allied Topics, Palm Springs, CA, June 1997. "The Use of Affinity Profiling Methodologies for Lead Candidate Selection"; Robyn A. Rourick, Michael L. Nedved, Neelanjana Ray, Mark E. Hail, Kevin J. Volk, Edward H. Kerns, and Mike S. Lee; 45th ASMS Conference on Mass Spectrometry and Allied Topics, Palm Springs, CA, June 1997. "Rapid, Automated LC/MS Methods for Protein Sample Cleanup and Characterization"; Mark E. Hail, Michael L. Nedved, Bethanne M. Warrack, William L. Thompson, Mike S. Lee; 10th Symposium of the Protein Society, San Jose, CA, August 1996. "Automated On-Line LC/MS Methods for Protein Sample Cleanup and Characterization"; Mark E. Hail, Michael L. Nedved, Bethanne M. Warrack, William L. Thompson, Mike S. Lee; 44th ASMS Conference on Mass Spectrometry and Allied Topics, Portland, OR, May 1996. "Automated High Throughput LC/MS for the Rapid Profiling of Pharmaceutical Compounds"; Mark E. Hail, Bethanne M. Warrack, Anne S. Arroyo, Gerald C. DiDonato, Mike S. Lee; 44th ASMS Conference on Mass Spectrometry and Allied Topics, Portland, OR, May 1996. "Using Scientific Visualization Software to Analyze Structural Trends in LC/MS Profile Datasets"; Jeffrey L. Whitney, Mark E. Hail, Robyn A. Rourick, Kevin J. Volk, Edward H. Kerns, Mike S. Lee; presented at 44th ASMS Conference on Mass Spectrometry and Allied Topics, Portland, OR, May 1996. "Investigation of the Production of cADPR and cGDPR by ADP-Ribosyl Cyclase using Electrospray Ionization Liquid Chromatography/Mass Spectrometry"; Bethanne M. Warrack, Mark E. Hail, David W. Green, Paulina Wang; presented at 44th ASMS Conference on Mass Spectrometry and Allied Topics, Portland, OR, May 1996. "A Novel Derivatization Scheme for the Collisional Activation of Peptides"; Rich E. Gedamke, Mark E. Hail, Gerald C. DiDonato, Mike S. Lee; presented at 44th ASMS Conference on Mass Spectrometry and Allied Topics, Portland, OR, May 1996. "Rapid Structural Analysis of Combinatorial Synthesis Products in Drug Discovery Using Mass Spectrometry" Mark Hail, J. Whitney, B. Warrack, R. Gedamke, G. DiDonato, M. Lee, K. Volk, R. Rourick, E. Kerns; Eastern Analytical Symposium, Somerset, NJ, November 20, 1996. "Rapid Characterization of Proteins in Drug Discovery Using Electrospray Ionization Mass Spectrometry"; Mark Hail, Mid-Atlantic Research Meeting of ACS, Villanova, PA, May 23, 1996.
"Automated Mass Spectral Analysis of Small and Large Molecules"; Mark Hail, Connecticut Mass Spectrometry Discussion Group, Wallingford, CT, December 3, 1996.
"Separation and Manipulation of Proteins using Polymeric m-HPLC Columns On-line with Electrospray Ionization/Mass Spectrometry"; Mark E. Hail, Bethanne M. Warrack, Susan C. Taylor, Sam Baldwin, Ken Stoney, Mike S. Lee, 43rd ASMS Conference on Mass Spectrometry and Allied Topics, Atlanta, GA, May 1995.
"Rapid Molecular Weight Determination Using Electrospray Ionization Mass Spectrometry"; Rich Gedamke, Gerald C. DiDonato, Mark E. Hail, and Mike S. Lee; 43rd ASMS Conference on Mass Spectrometry and Allied Topics, Atlanta, GA, May 1995. "Rapid On-Line Desalting and Separation of Polypeptides for Characterization by Electrospray Ionization LC/MS"; Mark E. Hail, Bethanne M. Warrack, Gerald C. DiDonato, and Mike S. Lee; Third International Symposium on Mass Spectrometry in the Health and Life Sciences, San Francisco, CA, September, 1994. "Characterization of a New Atmospheric Pressure Ionization Interface for Liquid Chromatography/Mass Spectrometry", M. E. Hail and I. Mylchreest, 41st ASMS Conference on Mass Spectrometry and Allied Topics, San Francisco, CA, 1993. "Automated Peptide Mapping and Sequencing by LC/ESI/MS", K. Mock, I. Mylchreest and M. Hail, M. Sanders, M. Uhrich, I. Jardine, 41st ASMS Conference on Mass Spectrometry and Allied Topics, San Francisco, CA, 1993. "A Heated Capillary Atmospheric Pressure Ionization Source with an Atmospheric Pressure Chemical Ionization Interface", I. Mylchreest and M. E. Hail, 41st ASMS Conference on Mass Spectrometry and Allied Topics, San Francisco, CA, 1993. "Rapid Automated Determination of Molecular Weights and Structural Information of Drugs and Other Organic Compounds Using ESI and APCI", M. Hail, I. Mylchreest, K. Mock, M. Sanders, and M. Uhrich, 41st ASMS Conference on Mass Spectrometry and Allied Topics, San Francisco, CA, 1993. "New APCI Technology Enhances Pharmokinetic Studies in Biological Samples", I. Mylchreest, M. Hail, M. Sanders, A. Land, M. Uhrich, and M. Wakefield, 41st ASMS Conference on Mass Spectrometry and Allied Topics, San Francisco, CA, 1993. "Advanced Quadrupole Mass Spectrometry: Applications", M. E. Hail and I. Mylchreest, Pittsburgh Conference, Atlanta, GA, 1993. "New Technology for Coupling Atmospheric Pressure Ionization (ESI/APCI) to Quadrupole Mass Spectrometers for Routine High Sensitivity LC/MS", M. E. Hail, I. Mylchreest, M. Urich, and I. Jardine, 9th Symposium on Liquid Chromatography/Mass Spectrometry, Montreux, Switzerland, 1993. "Applications of an Improved Electrospray Ionization Interface for LC/MS and LC/MS/MS of Biopolymers", M. E. Hail and I. Mylchreest, 39th ASMS Conference on Mass Spectrometry and Allied Topics, Nashville, TN, 1991, 556-557. "Enhancements to an Electrospray Ionization Interface for a Triple Quadrupole Mass Spectrometer", I. Mylchreest and M. E. Hail, 39th ASMS Conference on Mass Spectrometry and Allied Topics, Nashville, TN, 1991, 316-317. "Peptide Sequence Mapping: Quadrupole and Quadrupole Ion Trap Analysis of Peptides and Proteins by Micro-packed Capillary Liquid Chromatography and Capillary Electrophoresis", M. E. Hail, J. Schwartz, I. Mylchreest, K. Seta, S. Lewis, J. Zhou, J. Liu, and M. Novotny, 38th ASMS Conference on Mass Spectrometry and Allied Topics, Tucson, AZ, 1990, 353-354. "Characteristics of RF-only Multipole Collision Cells" M. E. Hail, J. E. P. Syka, A. E. Schoen, G. C. Stafford, and K. P. Matuszak, Pittsburgh Conference, New York, NY, 1989.
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