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Novatia Sample Submission Form

To submit an analysis request, begin by downloading a blank routine sample submission sheet. Open the blank sheet in Microsoft Excel and enter the sample information and details of the analysis requested for each sample to be submitted. Fields requiring information will be highlighted on the Excel sheet. Please include comments about samples on the submission on the Excel sheet. Please do this by using the comments section (column N) of the Excel sample submission sheet that you are uploading. The sample submission sheet will tabulate the analysis requests and calculate the estimated cost. Save the sheet and proceed with Steps 1 through 4.  Select the Submit button at the bottom of the page and a confirmation will be presented summarizing the request with shipping instructions.  A confirmation will also be emailed to the contact entered in Step 3. (Check your spam folder if you have not received a confirmation email)

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  • Rush Services available for 100% additional cost
  • See Novatia website for detailed pricing information

NMR Sample Requirements:

  • 1D Standard Analysis: >1 mg
  • 1D Standard 13C Analysis: >50 mg
  • 2D Standard Analysis: >10 mg
  • Samples must be received in either a sealed vial or sealed Eppendorf tube. Solid samples received in cellophane or zip lock bags will not be accepted and new samples provided in the acceptable storage containers will be requested.

NMR Analysis Time:

  • Analysis results usually within 5 business days of sample receipt

NMR Results:

  • Standard PDF Plots with peak list and integration
  • Raw data available upon request

NMR Experiment Key:

  • Proton = Hydrogen
  • F_19 = Fluorine
  • P_31 = Phosphorus
  • C_13 = Carbon
  • C_13_DEPT = DEPT Carbon
  • STAN_1H_COSY_HSQC_HMBC = 2D analysis including 1D proton, COSY, HSQC, and HMBC
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  • Rush Services available for 100% additional cost
  • See Novatia website for detailed pricing information

Note: MW Confirmation refers to nominal mass only

MS Sample Requirements

  • Minimum sample amounts
    • Small Molecules
      • 50-100 ug (e.g. 1-2 mg/mL x 25-50 uL)
      • Ideal for small molecule routine work would be at least 50 microliters of 400 micromolar sample.
      • Small molecule samples must be received in either a sealed vial or sealed Eppendorf tube. Solid samples received in cellophane or zip lock bags will not be accepted and new samples provided in the acceptable storage containers will be requested.
    • Oligonucleotides
      • Submit > 1 nmol if sending an oligonucleotide for oligo sequencing
      • Submit > 50 pico moles for oligo analyses. An ideal oligo submission for routine work would be at least 30 microliters of 5 micromolar sample
    • Proteins/ Peptides
      • 50-100 ug (e.g. 2 mg/ mL x 25-50 uL) for peptide mapping
      • 20-40 ug (e.g. 2 mg/mL x 10-20 uL) for Native MS methods
      • 10-20 ug (e.g. 1 mg/mL x 10-20 uL) for all other protein/peptide analysis.
  • Samples can be dry or lyophilized sample (specify grams or moles) or in solution (specify volume & concentration)
  • If the samples contain any detergent (Tween, TritonX, etc) tell us in the comments and provide an estimated concentration.
  • Provide target molecular weight, molecular formula, or structure.
    • Oligonucleotide sequences (use IDT designation as specified at IDT Oligo Nomenclature) this includes sequence modifications if they are available. If the modification is unique please provide a molecular formula or structure.
  • If submitting a small molecule, please indicate the structure and/or functional groups, a solvent, and any other important information in the Comments field of the Excel sheet

Plate Submission Notes:

MS Analysis Time:

  • MW Confirmation usually within 1 business day of sample receipt
  • Purity Profile usually within 2 business days of sample receipt
  • High Resolution data usually within 1-5 business days of sample receipt
  • Large quantities of samples may take longer

MS Results:

Click here to show Terms and Conditions

ROUTINE ANALYSIS TERMS AND CONDITIONS:

  1. Typical turnaround time is 1-5 business days for most analyses. Rush service moves your submission to the front of the instrument queue for 2X charge. Nominal mass oligonucleotides and 1D NMR usually same day or next day. Large numbers of samples may take longer.
  2. Payment for services will be made by check, credit card, wire transfer or ACH.  An approved purchase order (Net 30) or credit card details will be provided to Novatia upon submitting an analysis request: http://www.enovatia.com/novatia-sample-submission-form/ When paying by credit card, transactions will process at the time service is provided. Invoices are due and payable within the time noted on the invoice, measured from the date of the invoice.
  3. Work is NOT performed under regulated conditions (e.g. cGxP) and is “for information only.”
  4. Customer represents that submitted samples do not warrant exceptional handling or precautions (e.g., as with radioactive samples, controlled substances, highly potent or cytotoxic compounds, etc.) and that any available safety information (safety data sheet, occupational exposure level, control banding, etc.) will be relayed to Novatia prior to sample shipment.
  5. After analysis, customer will receive an email to view results on Novatia’s Secure Web Portal: Most MS results are ProMass HTML or ACD PDF report;  NMR results include ACD PDF report and zip file of raw NMR data.
  6. If additional custom data interpretation/reporting is required (apart from what is explicitly included in Point 5), Novatia can provide a quote to the customer at our hourly rate of $400/hr.
  7. Novatia does not retain samples after analysis. If sample return is required this must be requested at the time of the submission using the sample submission Excel sheet.